Crystal Structure of [Bi13 1/3[]2/3 Cu2O16](SO4)6.
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SYNTHESIS AND CRYSTAL STRUCTURE OF [PPh ] [WOS (CUNCS) ]
The reaction of [PPhJ, NOS,] with CuCl and KSCN (1 :3:3) in acetone produces the yell-ow crystals of [PPh,], [WOS,(CuNCS),]. The crystals are triclinic, space group P1(2), z=2, a=12.4823(7), b=12.9224(7), c=18.6395(10)?, ?=83.907(5), ?= 73.152(4), Y= 65.194(4)'. The crystal structure was determined by single crystal Xray diffraction methods (Mo-K ?) and refined by least-squares calculations ...
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ژورنال
عنوان ژورنال: Acta Chemica Scandinavica
سال: 1991
ISSN: 0904-213X
DOI: 10.3891/acta.chem.scand.45-0769